The bottom composition of a pilot-scale, methanol–water distillation column is measured using an on-line gas chromatograph (GC). The composition measurement is sent to a PI controller that adjusts the steam flow rate to the reboiler. Recently, the control-loop performance has deteriorated: the closed-loop composition response is more oscillatory and the period of oscillation is much larger than usual. The troubleshooting strategy used in Example 12.9 has indicated that neither a cyclic disturbance nor a sticking control valve is the source of the problem. According to the maintenance records, the filter in the sample line has been replaced recently. Suggest additional diagnostic tests that should be considered before controller re-tuning is performed as a last resort.